EPA-OW: NRSA Microcystins 2013 (Wade):  Microcystin (alga toxin) sample collection in small wadeable streams

  • Summary
  • Analytes
  • Revision
  • Data and Sites
Official Method Name
Section 9: Wadeable streams-Microcystins (of National Rivers and Streams Assessment: Field Operations Manual (2013))
Current Revision
2013
Media
WATER  (Waterbody type - Wadeable stream)
Instrumentation
Field Equipment
Method Subcategory
Microbiological
Method Source
  EPA-OW
Citation
  National Rivers and Streams Assessment 2013/14: Field Operations Manual–Wadeable
Protocol
EPA-841-B-12-009 - National Rivers and Streams Assessment: Field Operations Manual (2013)
Brief Method Summary
The microcystin (algal toxin) sample is a grab sample taken from the index site. All field crews must collect a grab sample using the 3 L beaker to fill a 500ml bottle. Collect this sample after the in situ measurements and water chemistry samples are collected. Store all samples on ice in a closed cooler.
Scope and Application
Methods described in this document are to be used specifically in work relating to the National Rivers and Streams Assessment. This document contains proceedures for how to collect a microcystin sample.
Applicable Concentration Range
Interferences
Quality Control Requirements
Follow outlined rinse proceedures.
Sample Handling
Samples must be kept cool and dark.
Maximum Holding Time
Relative Cost
Unknown
Sample Preparation Methods
Freeze the entire sample and keep frozen until shipping.