EPA-NERL: 210.1: Beryllium by Flame AA
Official Method Name
|
Beryllium (Atomic Absorption, Direct Aspiration) |
---|---|
Current Revision
| Issued 1974 |
Media
|
WATER |
Instrumentation
|
Flame Atomic Absorption |
Method Subcategory
|
Inorganic |
Method Source
|
|
Citation
|
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Brief Method Summary
|
A sample prepared according to EPA Method 200.0 is analyzed using a flame atomic absorption spectrometer. Specifications for instrument operation and preparation of standards are provided in the method. |
Scope and Application
|
This method determines beryllium by flame atomic absorption spectrometry. Sample pretreatment according to EPA Method 200.0 determines the applicability. |
Applicable Concentration Range
|
50-2,000 ug/L (optimal range); 25 ug/L (sensitivity). |
Interferences
|
(A) Sodium and Silicon: Sodium and silicon concentrations in excess of 1000 mg/L severely depress beryllium absorbance. (B) Bicarbonate ion: Bicarbonate ion can interfere, but is eliminated when samples are acidified to pH of 1.5. (C) Aluminum: Aluminum at 500 ug/L can depress the sensitivity of beryllium. For additional interferences see EPA Method 200.0. |
Quality Control Requirements
|
QC requirements for drinking water procedures are provided in method 200.0. |
Sample Handling
|
Sample handling and preservation procedures are provided in EPA Method 200.0. |
Maximum Holding Time
|
6 months (MCAWW, Table 1). |
Relative Cost
|
Less than $50 |
Sample Preparation Methods
|
200.0 |