USGS-OWQ: NFM 6.2.1-Lum:  Dissolved-oxygen concentration, field measurement by luminescent sensor

  • Summary
  • Analytes
  • Revision
  • Data and Sites
Official Method Name
Dissolved Oxygen, Luminescent-Sensor Method
Current Revision
Completed 01/24/2006
Media
WATER
Instrumentation
Luminescence Sensor
Method Subcategory
Inorganic
Method Source
  USGS-OWQ
Citation
  National Field Manual for the Collection of Water-Quality Data: U.S. Geological Survey Techniques of Water-Resources Investigations, Book 9, Chap. A6.2 "Dissolved Oxygen"
Brief Method Summary
Dissolved-oxygen measurement in natural water must be made in situ at the field site. The luminescent-sensor method specifies use of an instrument based on luminescent-sensor technology. The instrument calibration should be checked periodically in accordance with section 6.2.1B of the source citation. For surface-water measurements, the DO determination must be made in situ; refer to TWRI Book 9 Ch. A6.0 and Ch. A4 for isokinetic and nonisokinetic sampling methods. For ground-water measurements, the measurement must be made either downhole (in situ) at the given sampling interval, or within an air-tight flow-through chamber (cell) to which the sample is pumped directly from the downhole sampling interval; refer to TWRI Book 9 Ch. A6.0 and Ch. A4.2 for downhole and flow-through-chamber sampling methods.
Scope and Application
This method covers the measurement of dissolved oxygen (DO) concentrations in surface water and ground water using luminescent-sensor technology. Standard USGS surface-water measurements represent the median or mean in-situ value of a reach cross section. Standard ground-water measurements are made either in situ (downhole) or pumped directly to flow-through cell to exclude contact with air.
Applicable Concentration Range
1.0 to 20
Interferences
There are no known sources of interference to this method when used in situ in natural aquatic systems.
Quality Control Requirements
Calibration checks are strongly recommended.
Sample Handling
Measurements in surface water must be made in situ. Measurements in ground water are made either in situ (downhole) or in source water pumped into a flow-through cell, with sample temperature maintained constant from source to cell and excluding bubbles or other source of air.
Maximum Holding Time
zero holding time
Relative Cost
Unknown
Sample Preparation Methods
not applicable